Cis-2-Aminocyclohexanol Hydrochloride
Cis-2-Aminocyclohexanol Hydrochloride
CAS: 6936-47-6
Molecular Formula: C6H14ClNO
Cis-2-Aminocyclohexanol Hydrochloride - Names and Identifiers
Cis-2-Aminocyclohexanol Hydrochloride - Physico-chemical Properties
| Molecular Formula | C6H14ClNO |
| Molar Mass | 151.63 |
| Melting Point | 186-190 °C |
| Appearance | Crystalline Powder |
| Color | White to slightly beige |
| Storage Condition | Inert atmosphere,Room Temperature |
Cis-2-Aminocyclohexanol Hydrochloride - Risk and Safety
| Risk Codes | R36/37/38 - Irritating to eyes, respiratory system and skin. R41 - Risk of serious damage to eyes R37/38 - Irritating to respiratory system and skin. R22 - Harmful if swallowed |
| Safety Description | S37/39 - Wear suitable gloves and eye/face protection S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S39 - Wear eye / face protection. |
| HS Code | 29221990 |
Cis-2-Aminocyclohexanol Hydrochloride - Reference Information
| Preparation | Cis-2-aminocyclohexanol hydrochloride is prepared as follows: 1) Cyclohexene (5.00g;51.99mmol) is slowly added to a mixture of cooled m-chloroperbenzoic acid (9.87g;57.19mmol) in 125ml CH2Cl2. The reaction mixture was gradually warmed to room temperature overnight. The mixture was filtered, washed with concentrated NaHCO3 and concentrated in vacuum to obtain light yellow oily cycloheptene oxide, which is directly used in the next step. 2) In a sealed tube, cyclohexene oxide (5.44g;48.50mmol) and ammonium hydroxide solution (10ml) in 4ml of methanol are heated to 80°C for 72 hours. After removing the heat, the mixture was vacuum concentrated to obtain cis-2-aminocyclohexanol hydrochloride. |
| application | cis-2-aminocyclohexanol hydrochloride can be used as an intermediate in pharmaceutical synthesis. |
Last Update：2024-04-09 21:01:54
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